Search results for " ToM"

Fast-ADT: A fast and automated electron diffraction tomography setup for structure determination and refinement.

2020

Abstract Electron crystallography has focused in the last few years on the analyses of microcrystals, mainly organic compounds, triggered by recent publications on acquisition methods based on direct detection cameras and continuous stage tilting. However, the main capability of a transmission electron microscope is the access to features at the nanometre scale. In this context, a new acquisition method, called fast and automated diffraction tomography (Fast-ADT), has been developed in form of a general application in order to get the most of the diffraction space from a TEM. It consists of two subsequent tilt scans of the goniometric stage; one to obtain a crystal tracking file and a secon…

Automated Diffraction Tomography for the Structure Elucidation of Twinned, Sub-micrometer Crystals of a Highly Porous, Catalytically Active Bismuth M…

2012

Joint interpretation of seismic refraction tomography and electrical resistivity tomography by cluster analysis to detect buried cavities

2020

Abstract In the last few years, the geophysical methods of seismic refraction tomography (SRT) and electrical resistivity tomography (ERT) are among the most used geophysical techniques for the reconstruction of subsoil geometries, for the investigation of underground cavities and also for the archaeological prospecting. However, the main disadvantage of each geophysical method is the difficulty of final interpretation of the data. In order to eliminate artifacts and generally improve the reliability and accuracy of geophysical interpretation, it is useful to perform a joint approach of different geophysical methods, also introducing the a priori information. In this work, it is shown the i…

Volcanic structures investigation through SAR and seismic interferometric methods: The 2011-2013 Campi Flegrei unrest episode

2019

Observations from satellites provide high-resolution images of ground deformation allowing to infer deformation sources by developing advanced modeling of magma ascent and intrusion processes. Nevertheless, such models can be strongly biased without a precise model of the internal structure of the volcano. In this study, we jointly exploited two interferometric techniques to interpret the 2011–2013 unrest at Campi Flegrei caldera (CFc). The first is the Interferometric Synthetic Aperture Radar (InSAR) technique, which provides highly-resolved spatial and temporal images of ground deformation. The second is the Ambient Noise Tomography (ANT), which images subsurface structures, providing the…

Essential features of the polytypic charoite-96 structure compared to charoite-90

2011

AbstractCharoite, ideally (K,Sr,Ba,Mn)15–16(Ca,Na)32[(Si70(O,OH)180)](OH,F)4·nH20, is a rock-forming mineral from the Murun massif in Yakutia, Sakha Republic, Siberia, Russia, where it occurs in a unique alkaline intrusion. Charoite occurs as four different polytypes, which are commonly intergrown in nanocrystallme fibres. We report the structure of charoite-96(a =32.11(6),b =19.77(4),c =7.23(1) Å, β = 95.85(9)°,V =4565(24) Å3, space groupP21/m),which was solvedab initioby direct methods on the basis of 2676 unique electron diffraction reflections collected by automated diffraction tomography and refined toR1/wR2=0.34/0.37. The structure of charoite-96 is related to that of the charoite-90,…

Geophysical prospection of the Roman city of Pollentia, Alcúdia (Mallorca, Balearic Islands, Spain)

2016

Abstract We present the results of the geophysical investigation carried out in the Roman city of Pollentia, in the island of Mallorca. The ancient city was identified in the 19th century. Old and new archaeological excavations have helped to uncover a residential area, a theatre, the forum, several necropolises and other remains of the city, but a large unexplored area has still to be investigated. For instance, the limits of the ancient town and the presence of harbour structures are still unknown. The geophysical survey has covered an area of more than 20.000 m2 by integrating magnetic, electromagnetic, electrical and ground penetrating radar (GPR) methods. Many unseen archaeological fea…

The river harbour of Ostia Antica - stratigraphy, extent and harbour infrastructure from combined geophysical measurements and drillings

2018

Abstract We performed a combined geophysical and geoarchaeological survey of the harbour of ancient Ostia, Italy, to investigate the extent of the former harbour basin, the sedimentary infill and possible building remains around the harbour. Besides geoarchaeological results the paper highlights the advantage of combining vibracore drilling with different geophysical prospection methods, which are sensitive to different physical soil parameters. Geophysical methods applied were electrical resistivity tomography (ERT), ground penetrating radar (GPR) and seismics with shear and compressional waves. The extent and shape of the harbour basin were determined by ERT profiling. The ERT profiles we…

2018

The Yellowstone magmatic system is one of the largest magmatic systems on Earth, and thus an ideal location to study magmatic processes. Whereas previous seismic tomography results could only image...

Minimally invasive bone biopsies of fully wrapped mummies guided by computed tomography and fibre-optic endoscopy: Methods and suggested guidelines

2020

Abstract Recent advances in the recovery and analysis of ancient DNA (aDNA) and application of isotopic analysis of tissue obtained from mummified human remains has been accompanied by continued advances in non-invasive imaging using X-ray computed tomography (CT) and use of minimally invasive surgical techniques employing small fibre-optic endoscopes. We used these state-of-the-art techniques to examine ancient Egyptian mummies in the Egyptian Museum and Papyrus Collection of Berlin, obtaining bone samples for aDNA, stable isotope analyses and radiocarbon dating. CT and endoscopic guidance were applied to locate and biopsy bones using pre-existing access points in order to avoid any furthe…

Combined Electrical Resistivity Tomography (ERT), Direct-Push Electrical Conductivity (DP-EC) Logging and Coring - A New Methodological Approach in G…

2016

Non-invasive geophysical methods have been increasingly applied in geoarchaeological research commonly showing the need of data calibration based on stratigraphical information deduced from outcrops or sediment cores. In this contribution, a methodological approach combining two-dimensional (2D) electrical resistivity tomography (ERT) and stratigraphical data based on coring and, for the first time in geoarchaeological research, direct-push electrical conductivity (DP-EC) logging is presented and discussed. The approach yields high resolution data based on studies of two different types of archives, the Holsterburg site in central Germany located in a fluvio-terrestrial zone and the Corfu C…